A new reaction vessel for accelerated syntheses using microwave dielectric super-heating effects

David R. Baghurst; D. Michael P. Mingos

doi:10.1039/DT9920001151

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Journal of the Chemical Society, Dalton Transactions

Issue 7, 1992

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A new reaction vessel for accelerated syntheses using microwave dielectric super-heating effects

David R. Baghurst and D. Michael P. Mingos

J. Chem. Soc., Dalton Trans., 1992, 1151-1155

DOI: 10.1039/DT9920001151

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Abstract
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Using a thick-walled glass reaction vessel a number of transition-metal organometallic and co-ordination compounds have been synthesised using microwave dielectric super-heating effects. Super-heating by 40–60 °C is maintained by controlling the pressure at 10 atm and results in a decrease in the reaction time required for conventional reflux reactions by a factor of ca. 10². Full details of the design of the apparatus, the modification of a conventional microwave oven and the electrical circuitry for the pressure control are provided.

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Journal of the Chemical Society, Dalton Transactions

A new reaction vessel for accelerated syntheses using microwave dielectric super-heating effects

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