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Issue 12, 1991
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Synthesis and characterisation of nona-osmium carbonyl clusters; crystal and molecular structure of [(Ph3P)2N][Os9H(CO)24]

Angelo J. Amoroso,  Brian F. G. Johnson,  Jack Lewis,  Paul R. Raithby  and  Wing Tak Wong 

Abstract

The anion [Os9H(CO)24]–, 2 has been isolated in moderate yield by the vacuum pyrolysis of [Os3(CO)10(NCMe)2], and has been shown by a single crystal X-ray structure analysis to contain the previously unobserved tricapped octahedral Os9 metal core.

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Article type: Paper
DOI: 10.1039/C39910000814
Citation: J. Chem. Soc., Chem. Commun., 1991,0, 814-815
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    Synthesis and characterisation of nona-osmium carbonyl clusters; crystal and molecular structure of [(Ph3P)2N][Os9H(CO)24]

    A. J. Amoroso, B. F. G. Johnson, J. Lewis, P. R. Raithby and W. T. Wong, J. Chem. Soc., Chem. Commun., 1991, 0, 814
    DOI: 10.1039/C39910000814

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