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Issue 9, 1988
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Two-step synthesis of D3 and C3h cryptophanes

Abstract

Dihalides X–(Z)–X, [Z =(CH2)n; n= 1–7 or CH2CH[double bond, length half m-dash]CHCH2] react with the phenol group of vanillyl alcohol to give the dialkylated derivatives HOCH2–Ar–O–(Z)–O–Ar–CH2OH (2), which in turn, in the presence of formic acid, afford the corresponding D3 cryptophanes (3), with, in some cases, minor amounts of the C3h isomers (4).

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Article type: Paper
DOI: 10.1039/C39880000582
Citation: J. Chem. Soc., Chem. Commun., 1988, 582-584
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    Two-step synthesis of D3 and C3h cryptophanes

    J. Canceill and A. Collet, J. Chem. Soc., Chem. Commun., 1988, 582
    DOI: 10.1039/C39880000582

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