An enantiospecific synthesis of the dioxygenated spiroacetal moiety of milbemycins α7 and α8 has been developed from the appropriate epoxide and regioselective acylation of the C-23 alcohol.
R. Baker, C. J. Swain and J. C. Head, J. Chem. Soc., Chem. Commun., 1986, 874 DOI: 10.1039/C39860000874
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