Mercurated and tellurated Schiff bases and phenylhydrazones

Harkesh B. Singh; William R. McWhinnie

doi:10.1039/DT9850000821

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Journal of the Chemical Society, Dalton Transactions

Issue 4, 1985

The international journal for inorganic, organometallic and bioinorganic chemistry

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Mercurated and tellurated Schiff bases and phenylhydrazones

Harkesh B. Singh and William R. McWhinnie

J. Chem. Soc., Dalton Trans., 1985, 821-825

DOI: 10.1039/DT9850000821

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Abstract
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Attempts directly to tellurate Schiff bases or phenylhydrazones result in ionic products arising from hydrolysis of tellurium tetrahalides. However use of mercurated Schiff bases and mercurated phenylhydrazones does afford tellurated derivatives on trans-metallation with tellurium tetrabromid or organotellurium trichlorides. [4-Methoxy-2-(phenyliminomethyl)phenyl-C¹,N]tellurium(IV) tribromide may be reduced in poor yield to the monobromide. Spectroscopic data (i.r., ¹H n.m.r.) are presented and discussed. In particular, ¹³C n.m.r. spectra were valuable to establish the position of mercuration of the phenylhydrazones.

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Mercurated and tellurated Schiff bases and phenylhydrazones

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