Transmission spectra below 450 cm–1 can be easily obtained from thin films (ca. 18 µm) of aqueous solutions with a multiple scan Fourier transform i.r spectrometer; a study of solutions with CI:TlIII ratios of 4·1–6·4, combined with interactive spectral substraction techniques, provides evidence for the existence of [TlCl5]2–.
C. Carr, P. L. Goggin and M. Sandström, J. Chem. Soc., Chem. Commun., 1981, 772 DOI: 10.1039/C39810000772
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