Heterocycles in organic synthesis. Part 22. The conversion of amines to thiocarbonate esters and thiocyanates

Alan R. Katritzky; Urban Gruntz; Nicola Mongelli; Marcos C. Rezende

doi:10.1039/P19790001953

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Journal of the Chemical Society, Perkin Transactions 1

Issue 0, 1979

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Heterocycles in organic synthesis. Part 22. The conversion of amines to thiocarbonate esters and thiocyanates

Alan R. Katritzky , Urban Gruntz , Nicola Mongelli and Marcos C. Rezende

J. Chem. Soc., Perkin Trans. 1, 1979, 1953-1956

DOI: 10.1039/P19790001953

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Primary amines with 2,4,6-triphenylpyrylium perchlorate give 1-substituted pyridinium perchlorates which with potassium ethyl xanthate readily produce S-alkyl-O-ethyl dithiocarbonates. Primary amines with 2.4,6-triphenylpyrylium thiocyanate form 1-substituted- 2,4,6-triphenylpyridinium thiocyanates which thermolyse smoothly to the corresponding alkyl and aralkyl thiocyanates

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Journal of the Chemical Society, Perkin Transactions 1

Heterocycles in organic synthesis. Part 22. The conversion of amines to thiocarbonate esters and thiocyanates

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