Initiation of olefin metathesis: reaction of deca-2,8-diene with catalysts formed from Me4Sn–WCl6 and Me3Al2Cl3–(Ph3P)2(NO)2Cl2Mo

Robert H. Grubbs; Charles R. Hoppin

doi:10.1039/C39770000634

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Journal of the Chemical Society, Chemical Communications

Issue 18, 1977

Journal of the Chemical Society, Chemical Communications was published between 1972 - 1995.

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Initiation of olefin metathesis: reaction of deca-2,8-diene with catalysts formed from Me₄Sn–WCl₆ and Me₃Al₂Cl₃–(Ph₃P)₂(NO)₂Cl₂Mo

Robert H. Grubbs and Charles R. Hoppin

J. Chem. Soc., Chem. Commun., 1977, 634-635

DOI: 10.1039/C39770000634

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Abstract
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The initial product of the metathesis of deca-2,8-diene with metathesis catalysts formed from either Me₄Sn–WCl₆ or Me₃Al₂Cl₃–(Ph₃P)₂(NO)₂Cl₂Mo is propene; labelling of the terminal groups of the diene and the alkylating agents gives a labelling pattern in the propene that is best explained in terms of generation of a carbene in the initiation step from the alkylating agent.

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Journal of the Chemical Society, Chemical Communications

Initiation of olefin metathesis: reaction of deca-2,8-diene with catalysts formed from Me₄Sn–WCl₆ and Me₃Al₂Cl₃–(Ph₃P)₂(NO)₂Cl₂Mo

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Journal of the Chemical Society, Chemical Communications

Initiation of olefin metathesis: reaction of deca-2,8-diene with catalysts formed from Me4Sn–WCl6 and Me3Al2Cl3–(Ph3P)2(NO)2Cl2Mo

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Initiation of olefin metathesis: reaction of deca-2,8-diene with catalysts formed from Me₄Sn–WCl₆ and Me₃Al₂Cl₃–(Ph₃P)₂(NO)₂Cl₂Mo