Novel approach to the high-yield synthesis of tertiary alcohols using organoboranes

Rosemary J. Hughes; Andrew Pelter; Keith Smith

doi:10.1039/C3974000863A

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Journal of the Chemical Society, Chemical Communications

Issue 21, 1974

Journal of the Chemical Society, Chemical Communications was published between 1972 - 1995.

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Novel approach to the high-yield synthesis of tertiary alcohols using organoboranes

Rosemary J. Hughes, Andrew Pelter and Keith Smith

J. Chem. Soc., Chem. Commun., 1974, 863a-863a

DOI: 10.1039/C3974000863A

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Abstract
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Trialkylmethanols (R¹₂R²COH) are produced in essentially quantitative yields by treatment of trialkylboranes successively in the same vessel with 1-lithio-1,1-bis(phenylthio)alkene (–30 to 20°), HgCl₂(–78 to 0°) and alkaline hydrogen peroxide (20°).

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Journal of the Chemical Society, Chemical Communications

Novel approach to the high-yield synthesis of tertiary alcohols using organoboranes

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