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The Raman spectrum of the complex XF4, 2SbF5 is consistent with the ionic formulation XeF3+,Sb2F11–, and the 19F n.m.r. spectrum of the complex in solution in antimony pentafluoride has an AB2 spectrum in the F-on-Xe region which may be unambiguously assigned to the XeF3+ ion.
R. J. Gillespie, B. Landa and G. J. Schrobilgen, J. Chem. Soc. D, 1971, 1543 DOI: 10.1039/C29710001543
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