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Issue 3, 1969
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Nitramines and nitramides. Part XIV. Application of nuclear magnetic resonance spectra to the problem of isomerism in ON-dialkylnitramines, with some observations on ON-dialkylnitrosohydroxylamines

Alex. H. Lamberton  and  H. M. Yusuf 

Abstract

1 H Nuclear magnetic resonance spectra provide evidence for the existence of ON-dialkylnitramines (RH:NO2R′) in geometrically isomeric forms, which do not appear to be readily interconvertible. The spectra of some isomeric dialkyl nitrosohydroxylamines [RN(NO)OR′ and RN(O):NOR′] suggest for the structure RN(NO)OR′ an easier interconversion of conformers than is observed in N-nitrosodialkylamines. No signs of rotational isomerism were observed at 35° in the alkoxyurethanes which were prepared as intermediates.

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Article type: Paper
DOI: 10.1039/J39690000397
Citation: J. Chem. Soc. C, 1969,0, 397-400
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    Nitramines and nitramides. Part XIV. Application of nuclear magnetic resonance spectra to the problem of isomerism in ON-dialkylnitramines, with some observations on ON-dialkylnitrosohydroxylamines

    Alex. H. Lamberton and H. M. Yusuf, J. Chem. Soc. C, 1969, 0, 397
    DOI: 10.1039/J39690000397

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