In attempts to prepare crystals of Fremy's salt K4[(SO3)2NO]2 suitable for X-ray structural analysis, it has been found that the salt exists in two distinct crystalline forms, monoclinic yellow-orange needles, and triclinic orange-brown rhombs respectively. We describe the results of an X-ray structural analysis of the triclinic form.
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Journal of the Chemical Society A: Inorganic, Physical, Theoretical
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