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In attempts to prepare crystals of Fremy's salt K4[(SO3)2NO]2 suitable for X-ray structural analysis, it has been found that the salt exists in two distinct crystalline forms, monoclinic yellow-orange needles, and triclinic orange-brown rhombs respectively. We describe the results of an X-ray structural analysis of the triclinic form.
R. A. Howie, L. S. D. Glasser and W. Moser, J. Chem. Soc. A, 1968, 3043 DOI: 10.1039/J19680003043
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